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Beilstein J. Org. Chem. 2012, 8, 448–455, doi:10.3762/bjoc.8.51
Graphical Abstract
Figure 1: Schematic diagram of the network of hydrogen bonds in the binding pocket of the complex between MBP...
Figure 2: 2-19F-Maltose reporter system: Nonstereoselective fluorine labeling at the 2-position of maltose le...
Scheme 1: Syntheses of maltose derivatives; reagents and conditions: (a) Ac2O, Pyr, 97%; (b) HBr, AcOH, 99%; ...
Scheme 2: Synthesis of the maltose- and galacto-type derivatives; reagents and conditions: (a) TBDMS-Cl, imid...
Figure 3: 1-D 19F NMR: Experimental demonstration of differential binding of gluco- and manno-type 2-F-labele...
Figure 4: 19F NMR expansion (of Figure 3) of the gluco-type region of the 2-F-maltose reporter system.
Figure 5: Competitive titration with the 2-F-maltose reporter system and 19F NMR: only the important section ...